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Cabort, Amel

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Cabort, Amel
Affiliation principale
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https://libra.unine.ch/handle/123456789/389

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  • Publication
    Métadonnées seulement
    [RuCl{2,6-bis(3,4-dihydro-2H-pyrrol-5-yl)pyridine}(PPh3)2]BF4 dichloromethane solvate
    (2002)
    Cabort, Amel 
    ;
    Therrien, Bruno 
    ;
    Bernauer, Klaus
    ;
    Süss-Fink, Georg 
    The tetrafluoroborate salt of the mononuclear octahedral Ru(II) complex, [RuCl(L)(PPh3)2]BF4, where L = 2,6-bis(3,4-dihydro-2H-pyrrol-5-yl)pyridine, was prepd. as the CH2Cl2 solvate. Crystals are triclinic, space group P?1, with a 10.3368(8), b 12.7939(11), c 19.1336(16) Å, ? 80.231(10), ? 89.193(9), ? 67.943(9)°; Z = 2, dc = 1.505; R = 0.031, Rw(F2) = 0.076 for 8322 reflections. The PPh3 ligands adopt a trans configuration, with a P-Ru-P angle of 173.72(2)°. [on SciFinder(R)]